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Investigate the characterization of a compound of commercial or forensic significance with a molecular weight greater than 300 daltons.
1. Assemble the analytical data (LC, UV, IR, MS, NMR, etc) for this compound.
2. Propose fragments to account for any fragmentation observed in the MS spectrum.
3. For all of the 2D NMR experiments that were run COSY, HSQC, HMBC, etc. attempt to assign each cross-peak in each spectrum to the corresponding 1H-1H or 1H-13C correlation in the molecule.
4. Discuss the overall characterization of this molecule. Is all of the data consistent with the proposed structure? Explain.
5. Consider the following data. Propose a structure that is consistent with all of the data.
Data is attached
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